Method for obtaining antimicrobial flexible screen protectors for touch screens of electronic devices used in sensitive environments
                                                                                                                                                                                                                                                                                                                                 
PN-III-P2-2.1-PED-2019-4966
                                                                                                                                                       

Financial supported by Romanian Executive Agency for Higher Education, Research, Development and Innovation Funding (UEFISCDI)

Results 2022
Validation of the technology for the deposition of antimicrobial coatings on protective foils of mobile devices
  • Prototype of antimicrobial protective foils
Prototypes of protective foils for smart watches were obtained, using the most advanced antimicrobial coating obtained during the project. The protective foils were tested under normal use conditions, after application on smart watches.
  • Validated laboratory method for obtaining antimicrobial coatings
The laboratory method developed during the project was perfected and optimized during the last stage of the project. The method was validated by performing deposition of coatings both on laboratory samples, used for testing, and prototypes of protective foils, used for mobile devices.
  • Experimental model of antimicrobial coatings
Experimental model of antimicrobial coatings was obtained on polymer foils substrate.
  • Testing report on the functional characteristics
The functional characteristics of the protective foils were tested both on smart watches and on tablet. The touch screen capabilities were tested using a calibrated writing pen, proving that the coating does not affect the use of the device.
  • Characterization report for the antimicrobial activity of the coated foils, before and after ageing process
The time evolution of antimicrobial activity was followed over a period of 4 months, simulating the decay of activity due to storage. Moreover, the changes of the surface composition were described, following the testing procedures.
Attendance at international conferences
Oral presentations
  • Deposition And Characterisation Of Antimicrobial Thin Films On Transparent Polymer Foils By Magnetron Sputtering, Lidia R. Constantin, Anca C Parau, Adrian E. Kiss, Iulian. Pana, Mihaela Dinu, Alina Vladescu, Catalin Vitelaru, Cristina Adochite, Sarah Costinas, Mihaela Idomir, Mihaela Badea, Lavinia E. Tonofrei, “20th International Balkan Workshop on Applied Physics and Materials Science (IBWAP 2022)”, 12-15 July 2022, Constanta, Romania.
  • Synthesis and characterization of nanostructured silver based antibacterial coatings on protective polymer foils of touch screen devices, Catalin Vitelaru, Anca C. Parau, Adrian E. Kiss, Iulian Pana, Mihaela Dinu, Lidia R. Constantin, Alina Vladescu, Lavinia E. Tonofrei, Cristina S. Adochite, Sarah Costinas, Liliana Rogozea, Marius Moga, Mihaela E. Idomir, Mihaela Badea, The 6th International Conference New Trends on Sensing - Monitoring - Telediagnosis for Life Sciences NT-SMT-LS 2022”, 8-10 September 2022, Brasov, Romania.
  • The behavior of the medical staff and of the students from the Faculty of Medicine regarding the use of the mobile phone, Cristina Adochite, Mihaela Idomir, Sarah Costinas, Marius Moga, Liliana Rogozea, Daniela Neculoiu, Laura Floroia, Catalin Vitelaru, Anca C. Parau, Adrian E. Kiss, Iulian Pana, Mihaela Dinu, Lidia R. Constantin, Alina Vladescu, Mihaela Badea, The 6th International Conference New Trends on Sensing - Monitoring - Telediagnosis for Life Sciences NT-SMT-LS 2022”, 8-10 September 2022, Brasov, Romania.
Posters presentations
  • Combating Microbial Contamination With Silver-Based Transparent Coatings Obtained By Magnetron Sputtering On Polymer Foils- lucrare poster, L.R Constantin, A.C Parau, A.E. Kiss, I. Pana, M. Dinu, A. Vladescu, Catalin Vitelaru, Cristina Adochite, Sarah Costinas, Mihaela Idomir, Mihaela Badea, L.E. Tonofrei, „12th INTERNATIONAL CONFERENCE ON MATERIALS SCIENCE & ENGINEERING - BRAMAT 2022”, 9-11 March 2022, Brasov.
  • Method for obtaining antimicrobial flexible screen protectors for touch screens of electronic devices used in sensitive environments – MANTIFLEXIS, C. Vitelaru, A. C Parau, A. E. Kiss, I. Pana, M. Dinu, L R. Constantin, A. Vladescu, M. Badea, L. E. Tonofrei, « EUROPEAN EXHIBITION OF CREATIVITY AND INNOVATION - E U R O I N V E N T , 26-28 May 2022, Iasi – SILVER MEDAL and DIPLOMA OF EXCELLENCE AWARDS.
  • Method for obtaining antimicrobial flexible screen protectors for touch screens of electronic devices used in sensitive environments – MANTIFLEXIS, C. Vitelaru, A. C Parau, A. E. Kiss, I. Pana, M. Dinu, L R. Constantin, A. Vladescu, M. Badea, L. E. Tonofrei, « THE 26 th INTERNATIONAL CONFERENCE OF INVENTICS “INVENTICA 2022”, 23rd June – 24th June 2022, Iasi, Romania – SILVER MEDAL AWARD.
Published papers in ISI quoted journals
  • Silver-Containing Thin Films on Transparent Polymer Foils for Antimicrobial Applications, C. Vitelaru, A.C. Parau, A.E. Kiss, I. Pana, M. Dinu, L.R. Constantin, A. Vladescu, L.E. Tonofrei, C.S. Adochite, S. Costinas, L. Rogozea, M. Badea, M.E. Idomir, Coatings,12 (2022) 1-14, doi: 10.3390/coatings12020170
  • Optical Properties and Stability of Copper Thin Films for Transparent Thermal Heat Reflectors, I. Pana, A.C. Parau, M. Dinu, A.E. Kiss, L.R. Constantin, C. Vitelaru, Metals, 12 (2022) 1-12, doi: 10.3390/met12020262
  • Synthesis and Investigation of Antibacterial Activity of Thin Films Based on TiO2-Ag and SiO2-Ag with Potential Applications in Medical Environment, C.S.. Adochite, C. Vitelaru, A.C. Parau, A.E. Kiss, I. Pana, A. Vladescu, S. Costinas, M. Moga, R. Muntean, M. Badea, M. Idomir, Nanomaterials, 12 (2022) 1-11, doi: 10.3390/nano12060902
Results 2021
Development of deposition method for obtaining antimicrobial coatings consisting and assessment of their antimicrobial efficiency
  • Experimental model of foils coated with antimicrobial samples
Three types of layers were obtained and characterised: Ag+SiO2, Ag +TIO2 and SiO2+TiO2 respectively
  • Characterisation report of oxide layers with Ag nano-sized clusters
The physical properties of the layers were investigated using X ray diffraction, atomic force microscopy, UV-VIS spectrophotometry, EDX. The presence of nanocrystalline Ag, uniformly dispersed in the oxide matrix was made evident
  • Report on antimicrobial activity of coated protective foils and the vacuum processed foils
The antimicrobial activity of the various types of coated samples and the samples processed in vacuum condition (plasma cleaning) was evaluated. Optimum testing conditions were identified, using E,Coli as contaminant. The best antimicrobial activity was identified for the samples containing Ag and SiO2
  • Characterisation report on the mechanical and functional properties
The changes induced by the deposition of the antibacterial layer were investigated. The recovery time after controlled nano-sctracth was investigated using nanoindentation technique. The sensitivity of the touch screen with and without the protective foil, covered with antibacterial coating was evaluated using an adapted foil cutting device, with controllable pattern design and applied pressure
  • Report on the changes induced by ageing
The changes induced by ageing, both natural “on shelf” an accelerated by wiping with cloth were evaluated, both in terms of physical properties and antimicrobial activity. A reduction of both the quantity of available active silver and potential antimicrobial activity is observed
  • Report on the awareness degree on the contamination risks
The questionnaire was applied to selected population of healthcare workers in hospital and general population. Factors that influence the contamination of the mobile phones were identified, depending on gender, duration of use, specific activities, the disinfection methods employed etc
Attendance at international conferences
Oral presentations
  • Antimicrobial silver-based coatings obtained by magnetron sputtering on soft transparent polymers foils C. Vitelaru A.C Parau, A.E. Kiss, I. Pana, M. Dinu, L.R. Constantin, A. Vladescu, S. Costinas, C.S. Adochite, M. Moga, L. Floroian, M. Badea, M. Idomir, L.E Tonofrei, E-MRS 2021 Fall Meeting., Symposium J, 20-23 September 2021, Online
Posters presentations
  • Silver containing transparent films on polymer substrates for antimicrobial applications C. Vitelaru, A.C Parau, A.E. Kiss, I. Pana, M. Dinu, L.R Constantin, A. Vladescu, M.Badea, L.E. Tonofrei, 19th International conference on plasma physics and applications cppa 2021, August 31-September 3, 2021 Magurele-Bucharest, Romania
Published papers in ISI quoted journals
  • Silver containing thin films on transparent polymer foils for antimicrobial applications, C. Vitelaru, A.C. Parau, A.E. Kiss, I. Pana, M. Dinu, L.R. Constantin, A. Vladescu, L.E Tonofrei, C. Adochite, S. Costinas, L. Rogozea, M. Badea, M. Idomir, submitted to Coatings
  • Optical properties and stability of copper thin films for trans-parent thermal heat reflectors , Iulian Pana, Anca C. Parau, Mihaela Dinu, Adrian Emil Kiss, Lidia R. Constantin,and Catalin Vitelaru, submitted to Metals
Papers in other international journals
  • Strategies for in vitro testing of non-porous surfaces with antibacterial propertie, Cristina Adochițe , Sarah Costinaș , Mihaela Badea , Liliana Rogozea , Cătălin Vițelaru , Mihaela Idomir, Jurnal Medical Brasovean, no.1 -2021, 10.31926/jmb.2021.1.16
Results 2020
  • Definition of processing and testing conditions for the antimicrobial coatings
    • Experimental model of samples
    Custom made samples were prepared from self-adhesive polyurethane foils. The size and shape of the samples was defined and the cutting patterns were defined for the cutting machine. Experimental models of samples were obtained, having different shapes: circular or rectangular, with or without edges for manipulation
    • Characterisation report of antimicrobial activity of bare foils
    The testing conditions for antimicrobial activity were defined and implemented for the evaluation of antimicrobial activity of bare foils.
    • Report on selected processing conditions
    The vacuum compatibility of the substrate was checked and confirmed. The vacuum processing and plasma cleaning conditions were defined.
    • Experimental model of the deposition process for Ag nanostructures
    The process conditions for the deposition of Ag nanostructures were defined and characterised. HiPIMS was used as a deposition process, with tuneable frequency to obtain the desired deposition rate and amount of Ag.
    • Questionnaire for the evaluation of the public awareness on the contamination from mobile phones
    A questionnaire was defined to assess the awareness on the contamination from mobile phones.
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